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Beilstein J. Org. Chem. 2013, 9, 2022–2027, doi:10.3762/bjoc.9.238
Graphical Abstract
Scheme 1: Batch synthesis of NBDM. a) NaNO2, Amberlite IR-120 H+ (100 mL), 0 °C, water, 4 h. b) NH2OH·HCl, Na...
Scheme 2: The initial polymer-supported nitrite set up. A solution of glucosamine hydrochloride was passed ov...
Scheme 3: Continuous flow synthesis of the key intermediate 1-amino-2,5-anhydro-D-mannose (3).
Figure 1: Normalized NBDM absorption and emission, 40 µM and 2 µM.
Figure 2: NBDM fluorescence from 1–40 µM (PBS buffer). The data set was plotted in OriginPro 8.6 and fitted u...
Figure 3: Comparison of quenching 2 µM NBDM, as measured by fluorescence intensity of Trypan Blue, Bromopheno...
Figure 4: Comparison of quenching 2 µM NBDM, as measured by fluorescence intensity of methionine and histidin...